CHAPTER 4 SPECIAL METHODS This chapter will explain the methods used to measure the partitioning of elements to the gamma and gamma prime phases. The convergent beam diffraction method is one method described extensively in this chapter. Simple equations are developed which aid in interpreting the patterns and further allow simulated patterns of experimental patterns to be generated. The results of the lattice parameter measurements and strain measurements made using the CBED method are given in Chapter Five. Chapter Four also includes a brief section on energy dispersive analysis, specifically as it relates to the characterization of the alloys analyzed in this study. 4.1 Convergent Beam Electron Diffraction (CBED)Methods A convergent beam electron diffraction pattern is similar to a selected area diffraction pattern with one major and self-defining difference: a convergent beam pattern uses a focussed beam with a large convergence angle to define the area from which the diffraction 61