APPENDIX A HOLZ PATTERN CALCULATION Central to the calculations described in this appendix is the assumption that the microscope accelerating voltage can be arbitrarily defined. This will in turn define a relative crystal standard for the material that will be characterized. The standard operating voltage of the microscope is defined to be 100.00 KeV, for which the wavelength will be .037 Angstroms. For B=<114> and 9,3,1 diffracting planes, the resultant lattice parameter that exactly satisfies the equation in Section 4.1.3, is 3.5712 Angstroms. For the standard values just given, the four 9,3,1 HOLZ lines will intersect at a point in the center of the transmitted disc. The ratio of A to B (see Figure A) is referenced at this point to the values of Al and Bl given in the attached program listing. A larger or smaller lattice parameter will cause this ratio to vary. The ratio is listed as Rl in the table following the program. To account for noncubic effects, values of A3 and B3 are also calculated in the program. They are ratioed in the program and appear in the Table as the ratio R2. The values Tl, T2, etc. which appear in the program and in Figure A are delta theta-Bragg values, where delta