in binary alloys can these differences be accurately and unambiguously determined. Nevertheless, there are some generalizations that can be stated regarding the lattice parameter measurements and the partitioning effects in the RSR alloys. First, the lattice mismatch as measured by x-ray diffraction between the gamma and gamma prime phases is greater in the RSR 209 alloy than in the RSR 197 alloy. In both alloys, the gamma phase lattice parameter is greater than the gamma prime lattice parameter. The high Mo content in both alloys is responsible for this effect. In the Ta containing alloy, RSR 197, the gamma prime phase has a larger lattice parameter than the gamma prime phase in RSR 209. One interpretation of these observations is that the Ta, which substitutes readily for Al in the gamma prime phase, is the factor that increases the lattice parameter of the gamma prime in RSR 197. Nash and West (1979) report that about 8% Ta will increase the lattice parameter of gamma prime to about 3.59 Angstroms. The comparable unalloyed Ni3Al lattice parameter is about 3.57 Angstroms. The EDS data supports this Ta partitioning hypothesis since it was clearly shown that the Ta partitions predominantly to the gamma prime phase in RSR 197 under all the aging conditions in which it was measured. Thus, the local measurement of the gamma prime lattice parameter using the convergent beam technique can show the elemental partitioning differences in a