equal two. If U+V+W = odd, g-B will equal one. This calculation applies only to the first order zone. Most of the CBED patterns in this study were taken from the gamma prime phase, an L12 superlattice. In such a superlattice, the superlattice reflections appear in the forbidden positions for FCC. The true first order Laue zone for U+V+W = even will consist only of superlattice reflections. The first zone can be clearly seen in Figure 4.2, a B = (114> CBED pattern of the gamma prime phase in alloy RSR 197. These superlattice reflections are usually too weak to give HOLZ lines in the central disc. Only the HOLZ lines from the B = (114> "second" order zone were used in this study. This "second" zone will hereafter be referred to as the first order zone (FOLZ) since it in fact corresponds to the first order zone for a typical FCC crystal. An alternate way of deriving the preceding result is through construction of the Ewald sphere and geometrical solution of the intersection with the reciprocal lattice. With reference to Figure 4.3, the angle 0 equals 9' by similar triangles. Then Sin 9' = H/Igl/2R and Sin 9' = H/Igl. Combining these two equations gives g2 = 2RH. By definition, g2 = l/d2 = (h2+k2+12)/ao2. Substituting for igl2 gives h2+k2+12 = 2a2 RH. H can be shown to equal (g-B/a )(U2+V2+W2)1/2. Therefore, h2+k2+12 = (2aR/IBI)(g.B).