5.4 Energy Dispersive X-Ray Measurements....167 5.5 Microhardness Measurements.............. 167 6 DISCUSSION AND CONCLUSIONS................... 170 6.1 Metastable NixMo Phase Formation: Effects of Chemistry and Microstructure.......................... 170 6.2 Precipitation in RSR 197................176 6.3 Precipitation in RSR 209................179 6.4 Mechanical Response to Aging............179 6.5 Convergent Beam/X-Ray Diffraction.......181 6.6 Conclusions.............................183 REFERENCES. .................. .......................... 185 APPENDICES A HOLZ PATTERN CALCULATION.....................191 B INTERPLANAR ANGLES...........................199 BIOGRAPHICAL SKETCH.................................... 201